31,044 research outputs found

    Ion-retarding lens improves the abundance sensitivity of tandem mass spectrometers

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    Ion-retarding lens which increases the abundance sensitivity of tandem magnetic-analyzer mass spectrometers measures isotopes of low abundance in mass positions adjacent to isotopes of high abundance. The lens increases the abundance sensitivity for isotopes lying farther from high abundance isotopes than the energy cutoff of the lens

    Synthesis of hetero-bifunctional, end-capped oligo-EDOT derivatives

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    Conjugated oligomers of 3,4-ethylenedioxythiophene (EDOT) are attractive materials for tissue engineering applications, and as model systems for studying the properties of the widely used polymer PEDOT. We report here the facile synthesis of a series of keto-acid end-capped oligo-EDOT derivatives (n = 2-7) through a combination of a glyoxylation end capping strategy and iterative direct arylation chain extension. Importantly, these structures not only represent the longest oligo-EDOTs reported, but are also bench stable in contrast to previous reports on such oligomers. The constructs reported here can undergo subsequent derivatization for integration into higher order architectures, such as those required for tissue engineering applications. The synthesis of hetero-bifunctional constructs, as well as those containing mixed monomer units is also reported, allowing further complexity to be installed in a controlled manner. Finally, we describe the optical and electrochemical properties of these oligomers and demonstrate the importance of the keto-acid in determining their characteristics

    F-15 inlet/engine test techniques and distortion methodologies studies. Volume 7: Cross correlation functions.

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    Cross correlation function plots were used to determine if peak distortion data taken from a subscale inlet model can be used to predict peak distortion levels for a full scale flight test vehicle

    F-15 inlet/engine test techniques and distortion methodologies studies. Volume 3: Power spectral density plots

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    Power spectral density plots were used to determine if peak distortion data taken from a subscale inlet model can be used to predict peak distortion levels for a full scale flight test vehicle

    F-15 inlet engine test techniques and distortion methodologies studies. Volume 9: Stability audits

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    Stability audit plots were used to determine if peak distortion data taken from a subscale inlet model can be used to predict peak distortion levels for a full scale flight test vehicle

    F-15 inlet/engine test techniques and distortion methodologies studies. Volume 2: Time variant data quality analysis plots

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    Time variant data quality analysis plots were used to determine if peak distortion data taken from a subscale inlet model can be used to predict peak distortion levels for a full scale flight test vehicle

    F-15 inlet/engine test techniques and distortion methodologies studies. Volume 8: Cross spectral density plots

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    Cross spectral density plots were used to determine if peak distortion data taken from a subscale inlet model can be used to predict peak distortion levels for a full scale flight test vehicle

    F-15 inlet/engine test techniques and distortion methodologies studies. Volume 4: Autocorrelation functions

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    Autocorrelation function plots were used to determine if peak distortion data taken from a subscale inlet model can be used to predict peak distortion levels for a full scale flight test vehicle

    The enviornmental assessment of a contemporary coal mining system

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    A contemporary underground coal mine in eastern Kentucky was assessed in order to determine potential off-site and on-site environmental impacts associated with the mining system in the given environmental setting. A 4 section, continuous room and pillor mine plan was developed for an appropriate site in eastern Kentucky. Potential environmental impacts were identified, and mitigation costs determined. The major potential environmental impacts were determined to be: acid water drainage from the mine and refuse site, uneven subsidence of the surface as a result of mining activity, and alteration of ground water aquifers in the subsidence zone. In the specific case examined, the costs of environmental impact mitigation to levels prescribed by regulations would not exceed $1/ton of coal mined, and post mining land values would not be affected

    F-15 inlet/engine test techniques and distortion methodologies studies. Volume 5: Effect of filter cutoff frequency on turbulence plots

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    The effect of filter cutoff frequency on turbulence plots were used to determine if peak distortion data taken from a subscale inlet model can be used to predict peak distortion levels for a full scale flight test vehicle
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